HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ammonia → Octyl 4'-hydroxy-4-biphenylcarboxylate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ammonia | HCID 222 | — |
| Edukt | Dichloromethane | HCID 6344 | — |
| Edukt | Octyl4'-methoxycarbonyloxy-4-biphenylcarboxylate | HCID 18328376 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | Octyl 4'-hydroxy-4-biphenylcarboxylate | HCID 14692993 | — |
Reaktionsschritte
A solution of compound 5 (5.25 g, 0.014 mol) and aqueous ammonia (35% w/v, 100 ml) in ethanol (200 ml) was stirred for 1 h at room temperature. TLC analysis (dichloromethane) revealed a complete reaction. The solvent was removed in vacuo and the shite solid was recrystallised from ethanol to give colourless crystals.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06242636B1 |
| Quelldatensatz | uspto-grants-2001_06 |
| ORD ID | ord-4c0928ed998b44f0abc8a9f40a5bde1b |
| Quellennotiz | uspto-grants-2001_06 |