Trichloromethanesulfenyl chloride → Methyl[(trichloromethyl)sulfanyl]carbamyl fluoride

Reaktionsgleichung

[CH3:1][NH:2][C:3]([F:5])=[O:4].[Cl:6][C:7]([Cl:11])([Cl:10])[S:8]Cl.CCOP(OC1C=CC2C(C)=CC(OC=2C=1)=O)(OCC)=S>>[CH3:1][N:2]([S:8][C:7]([Cl:11])([Cl:10])[Cl:6])[C:3]([F:5])=[O:4]

Komponenten

Edukt 3

HCID 11666Trichloromethanesulfenyl chloride

HCID 10496498O,O-Diethyl O-(4-methyl-2-oxo-2H-1-benzopyran-7-yl) phosphorothioate

HCID 12545956Methylcarbamyl fluoride

Produkt 1

HCID 12836648Methyl[(trichloromethyl)sulfanyl]carbamyl fluoride

Versuchsvorschrift

N-Methyl-N-trichloromethanesulfenylcarbamoyl fluoride was prepared from methylcarbamoyl fluoride and trichloromethanesulfenyl chloride according to the method reported in West Germany Pat. No. 1.297,095 (Farbenfabriken Bayer, A. G), June 12, 1969.

Quellen und Nachweise

ORD-Eintrag: ord-0388dd647e5a431fb1044755311288ea
Quelldatensatz: uspto-grants-1976_05
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US03956500

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