HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sodium Hydroxide → Perilla alcohol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sodium Hydroxide | HCID 14798 | — |
| Edukt | Perillyl acetate | HCID 61780 | — |
| Produkt | Perilla alcohol | HCID 369312 | 97,7% |
Reaktionsschritte
Perillyl acetate (196 g.) derived from either of the examples mentioned and 30% aqueous sodium hydroxide (60 g.) were refluxed gently with stirring for 4 hours. The oil layer was separated and distilled under reduced pressure to give perillyl alcohol (150 g.) b.P. 80°/0.7 mm., αD20 + 102.5.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US03957856 |
| Quelldatensatz | uspto-grants-1976_05 |
| ORD ID | ord-39ae34768f2747dca013ecfce2e00257 |
| Quellennotiz | uspto-grants-1976_05 |