Phthalonitrile → Gallium phthalocyanine

HRID 1077993

Reaktionsgleichung

Reaktionsgleichung von HRID 1077993
[C:1](#[N:10])[C:2]1[C:3](=[CH:6][CH:7]=[CH:8][CH:9]=1)[C:4]#[N:5].C[O-].C[O-].C[O-].[Ga+3:17]>C(O)CO>[Ga:17].[CH:7]1[CH:8]=[CH:9][C:2]2[C:3](=[C:4]3[N:5]=[C:4]4[N:10]=[C:1]([C:2]5[CH:9]=[CH:8][CH:7]=[CH:6][C:3]=54)[N:10]=[C:1]4[NH:5][C:4]([C:3]5[CH:6]=[CH:7][CH:8]=[CH:9][C:2]=54)=[N:10][C:1]4=[N:5][C:4]([C:3]5[CH:6]=[CH:7][CH:8]=[CH:9][C:2]=54)=[N:10][C:1]=2[NH:5]3)[CH:6]=1

Komponenten

4

Edukt 2

HCID 7042PhthalonitrileHCID 131719385HCID 131719385, Verbindung

Produkt 1

HCID 136138306Gallium phthalocyanine

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 174Ethylene GlycolLösungsmittel

Versuchsvorschrift

31.8 parts of phthalonitrile, 10.1 parts of gallium trimethoxide and 150 ml of ethylene glycol were stirred under nitrogen atmosphere at 200° C. for 24 hours, and the product obtained was filtered. Then the product was washed with N,N-dimethylformamide and methanol successively, and dried to give 25.1 parts of gallium phthalocyanine.

Aufarbeitung

  1. customthe product obtained
  2. filtrationwas filtered
  3. washThen the product was washed with N,N-dimethylformamide and methanol successively
  4. customdried

Quellen und Nachweise

ORD-Eintrag
ord-77cc3d692a2e48d6b6625a27fe455e75
Quelldatensatz
uspto-grants-1996_08
Patentnummer
US05545733

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