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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1090793Erstellt: 26. Oktober 2026

Sodium Hydroxide → 4-(quinolin-2-ylmethoxy)benzoic Acid

https://huagongshe.com/reaction/1090793

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktSodium HydroxideHCID 14798—
EduktMethyl 4-(2-quinolinylmethoxy)benzoateHCID 19934817—
LösungsmittelEthanolHCID 702—
Produkt4-(quinolin-2-ylmethoxy)benzoic AcidHCID 983855265,5%

Reaktionsschritte

5.00 g of methyl-4-(quinolin-2-ylmethoxy)benzoate is dissolved in 120 ml of ethanol and 90 ml of 1N sodium hydroxide and the mixture is stirred at room temperature for 4 days. The mixture is concentrated in vacuo to remove the ethanol. The residue is diluted with water, acidified to pH 6 and the resulting solid is filtered off and recrystallized from methanol to give 3.12 g 4-(quinolin-2-ylmethoxy)benzoic acid.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05082849
Quelldatensatzuspto-grants-1992_01
ORD IDord-813a8b5498a34ca9a99a75095311e39c
Quellennotizuspto-grants-1992_01