Cesium fluoride → Allyl Oxalofluoride

HRID 1109259

Reaktionsgleichung

[CH2:1]([O:4][C:5](=[O:9])[C:6](Cl)=[O:7])[CH:2]=[CH2:3].[F-:10].[Cs+]>>[CH2:1]([O:4][C:5](=[O:9])[C:6]([F:10])=[O:7])[CH:2]=[CH2:3]

Komponenten

Edukt 2

HCID 25953Cesium fluoride

HCID 3018516Allyl chlorooxoacetate

Produkt 1

HCID 14153244Allyl Oxalofluoride

Versuchsvorschrift

By the procedure of the preceding Preparation, allyl oxalochloride (252.5 g, 1.70 mol) and cesium fluoride (284 g, 1.87 mol) were converted to twice distilled title product, b.p. 48°-50° C./35 mm; 124°-126° C. (atmospheric pressure).

Aufarbeitung

distillationto twice distilled title product, b.p. 48°-50° C./35 mm
custom124°-126° C. (atmospheric pressure)

Quellen und Nachweise

ORD-Eintrag: ord-f50bba0a23a44a65b38e743dc1911933
Quelldatensatz: uspto-grants-1994_06
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US05319103

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