Sulfuric Acid → 1-Amino-3,5-dimethyl-adamantane sulfate
Reaktionsgleichung
[NH2:1][C:2]12[CH2:11][C:6]3([CH3:12])[CH2:7][CH:8]([CH2:10][C:4]([CH3:13])([CH2:5]3)[CH2:3]1)[CH2:9]2.[S:14](=[O:18])(=[O:17])([OH:16])[OH:15]>CCOCC>[S:14]([OH:18])([OH:17])(=[O:16])=[O:15].[NH2:1][C:2]12[CH2:3][C:4]3([CH3:13])[CH2:10][CH:8]([CH2:7][C:6]([CH3:12])([CH2:5]3)[CH2:11]1)[CH2:9]2Komponenten
4
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
The dried ether solution of 1-amino-3,5-dimethyl-adamantane was treated with 0.5 gram concentrated sulfuric acid (H2SO4) in an ice bath, shaken, and the ether distilled. The oily residue was crystallized from hot water. Yield: 1.81 grams (80% of the theoretical yield).
Aufarbeitung
- distillationthe ether distilled