Benzoic acid, 4-(acetyloxy)- → p-Acetoxybenzoyl chloride
Reaktionsgleichung
[C:1]([O:4][C:5]1[CH:13]=[CH:12][C:8]([C:9](O)=[O:10])=[CH:7][CH:6]=1)(=[O:3])[CH3:2].C(Cl)(=O)C([Cl:17])=O>>[C:1]([O:4][C:5]1[CH:13]=[CH:12][C:8]([C:9]([Cl:17])=[O:10])=[CH:7][CH:6]=1)(=[O:3])[CH3:2]Komponenten
3
Versuchsvorschrift
A mixture of 4-acetoxybenzoic acid (516 mg) and oxalyl chloride (0.5 ml) was stirred for 30 minutes. The mixture was concentrated under reduced pressure to give 4-acetoxybenzoyl chloride.
Aufarbeitung
- concentrationThe mixture was concentrated under reduced pressure
Quellen und Nachweise
- ORD-Eintrag
- ord-a84bb63544524f4eb4575caeb8371555
- Quelldatensatz
- uspto-grants-2006_08
- Patentnummer
- US07098234B2
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