6-Methylbenzofuran → HCID 14257620, Verbindung

HRID 1194809Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1194809
[CH3:1][C:2]1[CH:10]=[CH:9][C:5]2[CH:6]=[CH:7][O:8][C:4]=2[CH:3]=1.[H][H]>CO.[Pd]>[CH3:1][C:2]1[CH:10]=[CH:9][C:5]2[CH2:6][CH2:7][O:8][C:4]=2[CH:3]=1

Komponenten

5

Edukt 2

HCID 869296-MethylbenzofuranHCID 178418361HCID 178418361, Verbindung

Produkt 1

HCID 14257620HCID 14257620, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 2

HCID 23938PalladiumKatalysatorHCID 887MethanolLösungsmittel

Versuchsvorschrift

6-Methylbenzofuran (15 g) was dissolved in methanol (200 ml) containing 0.5 g of 10% palladium on carbon. This solution was shaken on a Paar hydrogenator under hydrogen at 40 psi. When hydrogen uptake was complete, the solution was filtered through Celite and the ethanol evaporated to yield 6-methyl-2,3-dihydrobenzofuran.

Aufarbeitung

  1. filtrationthe solution was filtered through Celite
  2. customthe ethanol evaporated

Quellen und Nachweise

ORD-Eintrag
ord-ce17130a18534cd08a14dd4d6acf4092
Quelldatensatz
uspto-grants-1989_03
Patentnummer
US04816473

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