Benzoyl Peroxide → HCID 14368704, Verbindung
Reaktionsgleichung
[F:1][C:2]1[CH:11]=[C:10]([F:12])[CH:9]=[C:8]2[C:3]=1[CH:4]=[CH:5][CH:6]=[C:7]2[CH3:13].[Br:14]N1C(=O)CCC1=O.C(OOC(=O)C1C=CC=CC=1)(=O)C1C=CC=CC=1>C(Cl)(Cl)(Cl)Cl>[F:1][C:2]1[CH:11]=[C:10]([F:12])[CH:9]=[C:8]2[C:3]=1[CH:4]=[CH:5][CH:6]=[C:7]2[CH2:13][Br:14]Komponenten
5
Edukt 3
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
1.35 g of 5,7-Difluoro-1-methylnaphthaline in 10 ml of carbon tetrachloride are refluxed for 41/2 hours with 1.4 g of N-bromosuccinimide and 50 mg of dibenzoylperoxide. The cooled mixture is filtered and the solvent removed under vacuum. The purity of the crystalline crude product is sufficient for further reaction, m.p. 74°-76.5°.
Aufarbeitung
- filtrationThe cooled mixture is filtered
- customthe solvent removed under vacuum
- customThe purity of the crystalline crude product is sufficient for further reaction, m.p. 74°-76.5°
Quellen und Nachweise
- ORD-Eintrag
- ord-8c79336066a24a918e8010e041886d60
- Quelldatensatz
- uspto-grants-1992_05
- Patentnummer
- US05112851
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