[F:1][C@@H:2]([CH2:6][CH2:7][CH2:8][CH3:9])[CH2:3][CH2:4][OH:5].[CH3:10][S:11](Cl)(=[O:13])=[O:12]>N1C=CC=CC=1>[CH3:10][S:11]([O:5][CH2:4][CH2:3][C@@H:2]([F:1])[CH2:6][CH2:7][CH2:8][CH3:9])(=[O:13])=[O:12]To a 100 ml flask were added 8.7 g of (S)-3-fluoroheptanol and 21.5 g of pyridine in a nitrogen stream, and the solution was kept at 5° to 10° C. To the solution was added dropwise 7.5 g of methanesulfonyl chloride over 30 minutes, followed by stirring at 15° C. or less for 5 hours. The reaction mixture was poured into 200 ml of ice-water and extracted with ethyl acetate. The organic layer was washed successively with a diluted hydrochloric aqueous solution and water, dried over magnesium sulfate, and freed of the solvent by distillation at 30° C. or lower to obtain 12.7 g (93.18%) of the titled compound.
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