1,2-Epoxycyclododeca-5,9-diene → Cyclododecanol

HRID 1250040Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1250040
[O:1]1[CH:3]2[CH2:4][CH2:5][CH:6]=[CH:7][CH2:8][CH2:9][CH:10]=[CH:11][CH2:12][CH2:13][CH:2]12.[H][H]>[Pd]>[CH:2]1([OH:1])[CH2:13][CH2:12][CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3]1

Komponenten

4

Edukt 2

HCID 791351,2-Epoxycyclododeca-5,9-dieneHCID 178418361HCID 178418361, Verbindung

Produkt 1

HCID 15595CyclododecanolAusbeute 5 %

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 23938PalladiumKatalysator

Versuchsvorschrift

Also, the Drafted Report of 24th Symposium of Development in Reaction and Synthesis, Nov. 5 to 6, 1998, page 68, discloses a method of hydrogenating 1,2-epoxy-5,9-cyclododecadiene with hydrogen at ambient atmospheric pressure and room temperature in the presence of a catalyst comprising palladium carried on a carrier consisting of a carbon material. In this method, cyclododecanol was produced with a yield of 5% and no cyclododecanone was obtained.

Aufarbeitung

  1. customAlso, the Drafted Report of 24th Symposium of Development in Reaction and Synthesis, Nov
  2. customat ambient atmospheric pressure and room temperature

Quellen und Nachweise

ORD-Eintrag
ord-785d35ff3b6a41479bea5a07af8690e0
Quelldatensatz
uspto-grants-2002_01
Patentnummer
US06335472B1

Notizen zur Reaktion

Wird geladen…