Nitric Acid → Aluminum nitrate

HRID 1257483

Reaktionsgleichung

Reaktionsgleichung von HRID 1257483
[N+:1]([O-:4])([OH:3])=[O:2].O.O.O.O.O.O.O.O.O.[N+:14]([O-:17])([O-:16])=[O:15].[Al+3:18].[N+:19]([O-:22])([O-:21])=[O:20].[N+]([O-])([O-])=O>O>[N+:1]([O-:4])([O-:3])=[O:2].[Al+3:18].[N+:14]([O-:17])([O-:16])=[O:15].[N+:19]([O-:22])([O-:21])=[O:20]

Komponenten

4

Edukt 2

HCID 944Nitric AcidHCID 24567Aluminum nitrate nonahydrate

Produkt 1

HCID 26053Aluminum nitrate

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Versuchsvorschrift

An aqueous solution in which 4.16 kg of aluminum nitrate nonahydrate and 540 g of 60% nitric acid were dissolved in 5.0 L of pure water was gradually dropped into 20.0 kg of a stirred silica sol solution having a colloidal particle diameter of from 10 to 20 nm held at 15° C. (Snowtex N-30 manufactured by Nissan Chemical Industries, Ltd. (SiO2 content: 30% by mass)) to obtain a mixed slurry of silica sol and aluminum nitrate. Subsequently, the mixed slurry was aged by holding at 50° C. for 24 hours. After cooling to room temperature, the mixed slurry was spray-dried with a spray dryer set to an outlet temperature of 130° C. to obtain a solid.

Aufarbeitung

  1. additionwas gradually dropped into 20.0 kg of a stirred silica sol solution
  2. customheld at 15° C.

Quellen und Nachweise

ORD-Eintrag
ord-5f8bc8bd92e44bda9fadb8d56b7ccf97
Quelldatensatz
uspto-grants-2013_06
Patentnummer
US08461373B2

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