Perfluorooctanesulfonic acid → HCID 22726281, Verbindung

HRID 1265963

Reaktionsgleichung

Reaktionsgleichung von HRID 1265963
[F:1][C:2]([F:29])([S:25]([OH:28])(=[O:27])=[O:26])[C:3]([F:24])([F:23])[C:4]([F:22])([F:21])[C:5]([F:20])([F:19])[C:6]([F:18])([F:17])[C:7]([F:16])([F:15])[C:8]([F:14])([F:13])[C:9]([F:12])([F:11])[F:10].C(=O)([O-])[O-].[Ag+2:34]>O>[F:29][C:2]([F:1])([S:25]([O-:28])(=[O:27])=[O:26])[C:3]([F:23])([F:24])[C:4]([F:22])([F:21])[C:5]([F:19])([F:20])[C:6]([F:18])([F:17])[C:7]([F:16])([F:15])[C:8]([F:14])([F:13])[C:9]([F:12])([F:11])[F:10].[Ag+:34]

Komponenten

4

Edukt 2

HCID 74483Perfluorooctanesulfonic acidHCID 178418647HCID 178418647, Verbindung

Produkt 1

HCID 22726281HCID 22726281, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Versuchsvorschrift

Into a four-necked flask were charged 75 parts of perfluorooctanesulfonic acid and 100 parts of water, and 21.4 parts of silver carbonate was added thereto with stirring. After stirring at room temperature for 3 days, the mixture was filtered and the obtained filter-cake was washed with 10 parts of ion-exchange water, then 20 parts of diethylether and dried to give 60.3 parts of silver perfluorooctanesulfonate.

Aufarbeitung

  1. additionwas added
  2. stirringAfter stirring at room temperature for 3 days
  3. filtrationthe mixture was filtered
  4. filtrationthe obtained filter-cake
  5. washwas washed with 10 parts of ion-exchange water
  6. dry with material20 parts of diethylether and dried

Quellen und Nachweise

ORD-Eintrag
ord-6ac8754eaec44102a8cb06ad7b0bca55
Quelldatensatz
uspto-grants-2003_04
Patentnummer
US06548221B2

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