Ammonia → 3-Phenoxybenzyl 3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropanimidate

HRID 126978

Reaktionsgleichung

Reaktionsgleichung von HRID 126978
[Cl:1][C:2]([Cl:12])=[CH:3][CH:4]1[CH:6]([C:7]([NH2:9])=[O:8])[C:5]1([CH3:11])[CH3:10].ClC(Cl)=CC1C(C(O)=O)C1(C)C.C(Cl)(=O)C(Cl)=O.N.[O:32]([C:39]1[CH:40]=[C:41]([CH:44]=[CH:45][CH:46]=1)[CH2:42]Br)[C:33]1[CH:38]=[CH:37][CH:36]=[CH:35][CH:34]=1>>[Cl:1][C:2]([Cl:12])=[CH:3][CH:4]1[CH:6]([C:7](=[NH:9])[O:8][CH2:42][C:41]2[CH:44]=[CH:45][CH:46]=[C:39]([O:32][C:33]3[CH:38]=[CH:37][CH:36]=[CH:35][CH:34]=3)[CH:40]=2)[C:5]1([CH3:10])[CH3:11]

Komponenten

6

Edukt 5

HCID 222AmmoniaHCID 65578Oxalyl chlorideHCID 91658Permethric acidHCID 945441-(Bromomethyl)-3-phenoxybenzeneHCID 129533243-(2,2-Dichlorovinyl)-2,2-dimethylcyclopropanecarboxamide

Produkt 1

HCID 205713803-Phenoxybenzyl 3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropanimidate

Versuchsvorschrift

Following the method of Example 1, 3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropaneamide, from 3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropanecarboxylic acid, oxalyl chloride and ammonia, is reacted with 3-phenoxybenzyl bromide to give 3-phenoxybenzyl 3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropanimidate.

Quellen und Nachweise

ORD-Eintrag
ord-8ed25e8114b44f2dba6851bb4be38da4
Quelldatensatz
uspto-grants-1981_03
Patentnummer
US04254264

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