Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Benzoyl Peroxide | HCID 7187 | — |
| Edukt | Carbon tetrabromide | HCID 11205 | — |
| Edukt | Isooctyl acrylate | HCID 165746 | — |
| Edukt | Isobomyl acrylate | HCID 92004758 | — |
| Lösungsmittel | Ethyl Acetate | HCID 8857 | — |
| Produkt | Ioa iba | HCID 131723481 | — |
Reaktionsschritte
In a glass polymerization bottle were charged 80 g isooctyl acrylate (IOA), 18 g isobornyl acrylate (IBA), 2 g vinyldimethylazlactone (VDM), 100 g ethyl acetate, 0.5 g benzoyl peroxide and 0.04 g carbon tetrabromide. The bottle was purged with nitrogen, sealed and tumbled in a water bath maintained at 60° C. for 12 hours to produce a IOA/IBA/VDM terpolymer. The polymer was isolated by precipitation in isopropanol and dried under vacuum.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US06448337B1 |
|---|
| Quelldatensatz | uspto-grants-2002_09 |
|---|
| ORD ID | ord-0f178365228a4680a63c0489ca01ac42 |
|---|
| Quellennotiz | uspto-grants-2002_09 |
|---|
