Hydrochloric Acid → Benzenediazonium, 4-methoxy-, chloride

HRID 128002Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 128002
[N:1]([O-])=O.[Na+].[CH3:5][O:6][C:7]1[CH:12]=[CH:11][C:10]([NH2:13])=[CH:9][CH:8]=1.[ClH:14]>O>[Cl-:14].[CH3:5][O:6][C:7]1[CH:12]=[CH:11][C:10]([N+:13]#[N:1])=[CH:9][CH:8]=1

Komponenten

5

Edukt 3

HCID 313Hydrochloric AcidHCID 7732P-AnisidineHCID 23668193Sodium Nitrite

Produkt 1

HCID 11829892Benzenediazonium, 4-methoxy-, chlorideAusbeute 77 %

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel2×

Versuchsvorschrift

A solution of 4-methoxy-phenyl-diazonium chloride was prepared by adding dropwise at 0° C. a solution of 1.8 g of sodium nitrite dissolved in 2.5 ml of water to a solution of 3.075 g of p-anisidine dissolved in 25 ml of water and 8.1 ml of concentrated hydrochloric acid. The reaction mixture was allowed to stand for 2 hours.

Quellen und Nachweise

ORD-Eintrag
ord-3bf2fabb883b43b583957c7643dfea67
Quelldatensatz
uspto-grants-1981_03
Patentnummer
US04258120

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