1-Chloro-4-nitrobenzene → 2-(4-Aminophenoxy)ethanol
Reaktionsgleichung
[N+:1]([C:4]1[CH:13]=[CH:12][C:7]([O:8][CH2:9][CH2:10][OH:11])=[CH:6][CH:5]=1)([O-])=O.ClC1C=CC([N+]([O-])=O)=CC=1.C(=O)([O-])[O-].[Na+].[Na+]>C(O)CO>[NH2:1][C:4]1[CH:5]=[CH:6][C:7]([O:8][CH2:9][CH2:10][OH:11])=[CH:12][CH:13]=1Komponenten
5
Edukt 3
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
2-(4-Aminophenoxy)ethanol was prepared, using the method described in Example C3, by the reduction of 2-(4-nitrophenoxy)ethanol which was prepared by heating a mixture of 4-chloronitrobenzene, ethylene glycol and sodium carbonate in a sealed vessel (Beil. 6, II, 222).
Aufarbeitung
- customwas prepared
- temperatureby heating
Quellen und Nachweise
- ORD-Eintrag
- ord-15c442ca4f6c4400b134ad4f89e482c3
- Quelldatensatz
- uspto-grants-1995_11
- Patentnummer
- US05464781
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