Acetic Anhydride → HCID 20377231, Verbindung

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Reaktionsgleichung

[Cl:1][CH2:2][CH2:3][Si:4](Cl)(Cl)Cl.C([O:11][C:12](=[O:14])[CH3:13])(=O)C>>[Cl:1][CH2:2][CH2:3][Si:4]([O:11][C:12](=[O:14])[CH3:13])([O:14][C:12](=[O:11])[CH3:13])[O:14][C:12](=[O:11])[CH3:13]

Komponenten

Edukt 2

HCID 7918Acetic Anhydride

HCID 80386Trichloro(2-chloroethyl)silane

Produkt 1

HCID 20377231HCID 20377231, VerbindungAusbeute 80,5 %

Versuchsvorschrift

An amount of 40.8 g of 2-chloroethyl-trichlorosilane is dissolved in 71.5 g of acetic acid anhydride, and the solution allowed to stand at room temperature for 21 hours in a closed vessel. The reaction product is concentrated in vacuo to obtain 44.6 g of 2-chloro-ethyl-tris-(acetyloxy)-silane, B.P.: 85° - 88° /0.1 Torr, nD20 = 1.6687.

Aufarbeitung

concentrationThe reaction product is concentrated in vacuo

Quellen und Nachweise

ORD-Eintrag: ord-f36c1de8cde7409d882941b64f49d6ff
Quelldatensatz: uspto-grants-1976_10
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US03985780

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