Benzene → Phenylthionophosphonic dichloride

HRID 1288486

Reaktionsgleichung

Reaktionsgleichung von HRID 1288486
[P:1]([Cl:5])(Cl)([Cl:3])=[S:2].[CH:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1>>[C:6]1([P:1]([Cl:5])([Cl:3])=[S:2])[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1

Komponenten

3

Edukt 2

HCID 241BenzeneHCID 19883Thiophosphoryl chloride

Produkt 1

HCID 19016Phenylthionophosphonic dichloride

Reaktionsbedingungen

Temperatur
200 °C

Versuchsvorschrift

In a 100 cc autoclave, 42.35 g (0.25 mole) of thiophosphoryl trichloride, 19.53 g (0.25 mole) of benzene were charged, and the mixture was heated with stirring at 200° C for 4 hours. The reaction mixture was treated in accordance with the process of Example 1. No phenylphosphonothioic dichloride was produced.

Aufarbeitung

  1. temperaturethe mixture was heated
  2. additionThe reaction mixture was treated in accordance with the process of Example 1

Quellen und Nachweise

ORD-Eintrag
ord-3415756249a948d698066d8c2ad191f4
Quelldatensatz
uspto-grants-1976_10
Patentnummer
US03988368

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