Ibuprofen, (+-)- → HCID 15948295, Verbindung

HRID 1294405Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1294405
[OH:1][C:2]([CH:4]([C:6]1[CH:15]=[CH:14][C:9]([CH2:10][CH:11]([CH3:13])[CH3:12])=[CH:8][CH:7]=1)[CH3:5])=[O:3].[OH-].[Na+].O.O.O.O.O.O.[Cl-].[Sr+2:25].[Cl-]>O>[O-:3][C:2]([CH:4]([C:6]1[CH:7]=[CH:8][C:9]([CH2:10][CH:11]([CH3:12])[CH3:13])=[CH:14][CH:15]=1)[CH3:5])=[O:1].[Sr+2:25].[O-:3][C:2]([CH:4]([C:6]1[CH:7]=[CH:8][C:9]([CH2:10][CH:11]([CH3:12])[CH3:13])=[CH:14][CH:15]=1)[CH3:5])=[O:1]

Komponenten

5

Edukt 3

HCID 3672Ibuprofen, (+-)-HCID 14798Sodium HydroxideHCID 6101868Strontium chloride hexahydrate

Produkt 1

HCID 15948295HCID 15948295, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel2×

Versuchsvorschrift

Ibuprofen (2.59 g, 12.5 mmol) was dissolved in water (100 ml) containing sodium hydroxide (0.503 g, 12.5 mmol). A solution of strontium chloride hexahydrate (1.68 g, 6.3 mmol) in water (5 ml) was added. The mixture was stirred for 10 minutes at room temperature and the title compound was isolated by filtration and dried. Yield 1.30 g (44%). Melting point >300° C.

Quellen und Nachweise

ORD-Eintrag
ord-17ef2aaa02194c228bbb1d1cb414ffa2
Quelldatensatz
uspto-grants-2007_07
Patentnummer
US07241460B2

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