Butanal → 56249-61-7

HRID 1295424Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1295424
[CH:1](=O)[CH2:2][CH2:3][CH3:4].[CH2:6]([NH2:13])[C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1>C1(C)C=CC=CC=1>[CH:1](=[N:13][CH2:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1)[CH2:2][CH2:3][CH3:4]

Komponenten

4

Edukt 2

HCID 261ButanalHCID 7504Benzylamine

Produkt 1

HCID 455591156249-61-7

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 1140TolueneLösungsmittel

Versuchsvorschrift

This material is a known compound prepared in the standard fashion. To about 100 mL of toluene was added 28 mL of butyraldehyde, 34 mL of benzylamine, and several grams of 3A molecular sieves. The mixture became warm and turbid after standing for a few minutes. After standing for several hours the mixture was colorless and transparent. The imine product was isolated by distillation under vacuum and characterized by NMR spectroscopy.

Aufarbeitung

  1. customprepared in the standard fashion
  2. temperatureThe mixture became warm
  3. waitafter standing for a few minutes
  4. waitAfter standing for several hours

Quellen und Nachweise

ORD-Eintrag
ord-975dd027af1d4246842a1aa172023b42
Quelldatensatz
uspto-grants-2007_07
Patentnummer
US07241839B2

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