Lithium Hydroxide → Lithium 2,4,6-tris(dimethylaminomethyl)phenolate

HRID 129906Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 129906
[CH3:1][N:2]([CH2:4][C:5]1[CH:10]=[C:9]([CH2:11][N:12]([CH3:14])[CH3:13])[CH:8]=[C:7]([CH2:15][N:16]([CH3:18])[CH3:17])[C:6]=1[OH:19])[CH3:3].[OH-].[Li+:21]>>[CH3:3][N:2]([CH2:4][C:5]1[CH:10]=[C:9]([CH2:11][N:12]([CH3:13])[CH3:14])[CH:8]=[C:7]([CH2:15][N:16]([CH3:18])[CH3:17])[C:6]=1[O-:19])[CH3:1].[Li+:21]

Komponenten

3

Edukt 2

HCID 3939Lithium HydroxideHCID 70262,4,6-Tris((dimethylamino)methyl)phenol

Produkt 1

HCID 23711568Lithium 2,4,6-tris(dimethylaminomethyl)phenolateAusbeute 100,1 %

Versuchsvorschrift

Analogously to Example 19, starting from 53.1 g (0.2 mol) of 2,4,6-tris(dimethylaminomethyl)phenol and 9.2 g (0.2 mol) of lithium hydroxide there are obtained 54.3 g of lithium 2,4,6-tris(dimethylaminomethyl)phenolate in the form of an orange solid of which the elemental analysis is as follows:

Quellen und Nachweise

ORD-Eintrag
ord-23f3457368d942959f585299ed7f612f
Quelldatensatz
uspto-grants-1995_11
Patentnummer
US05470896

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