Ammonium Hydroxide → HCID 18506197, Verbindung

Reaktionsgleichung

[NH2:1][C:2]1[CH:19]=[CH:18][CH:17]=[CH:16][C:3]=1[O:4][C:5]1[CH:6]=[C:7]2[C:11](=[CH:12][CH:13]=1)[C:10](=[O:14])[NH:9][C:8]2=[O:15].[OH-].[NH4+:21]>>[NH2:1][C:2]1[CH:19]=[CH:18][CH:17]=[CH:16][C:3]=1[O:4][C:5]1[CH:6]=[C:7]([C:8]([NH2:21])=[O:15])[C:11](=[CH:12][CH:13]=1)[C:10]([NH2:9])=[O:14]

Komponenten

Edukt 2

HCID 14923Ammonium Hydroxide

HCID 18506076HCID 18506076, Verbindung

Produkt 1

HCID 18506197HCID 18506197, Verbindung

Versuchsvorschrift

5-(2-Aminophenoxy)-isoindole-1,3-dione (0.1 g, 0.38 mmol) in conc. ammonium hydroxide (aq) was stirred at 60° C. for two hours. The reaction mixture was evaporated in vacuo (cold in order not to make the imide again). The crude mixture was used without any purification.

Aufarbeitung

customThe reaction mixture was evaporated in vacuo (cold in order not
customThe crude mixture was used without any purification

Quellen und Nachweise

ORD-Eintrag: ord-fc642962978f4fe8bbdcf534f802d180
Quelldatensatz: uspto-grants-2003_07
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US06590118B1

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