Potassium Chloride → 3-(1-Methylpyrrolidin-2-yl)pyridine

HRID 1365588

Reaktionsgleichung

Reaktionsgleichung von HRID 1365588
[Cl-].[Na+].[Cl-].[K+].O=[CH:6][C@@H:7]([C@H:9]([C@@H:11]([C@@H:13]([CH2:15]O)O)O)O)O.[Cl-].[Ca+2].[Cl-].P([O-])(O)(O)=O.[K+].S([O-])([O-])(=O)=O.[Mg+2].[NH:32]([C:37]([CH2:42]O)(CO)CO)[CH2:33]C(O)=O.C1[N:49](CCCS(O)(=O)=O)[CH2:48]COC1.[OH-].[Na+]>>[N:49]1[CH:48]=[C:11]([CH:13]2[CH2:15][CH2:42][CH2:37][N:32]2[CH3:33])[CH:9]=[CH:7][CH:6]=1

Komponenten

9

Edukt 8

HCID 4873Potassium Chloride2×HCID 5234Sodium Chloride2×HCID 24083Sulfuric acid magnesium salt (1:1)2×HCID 79784TricineHCID 107526(2R,3S,4R,5R)-2,3,4,5,6-pentahydroxyhexanal2×HCID 516951Monobasic potassium phosphate2×HCID 5284359Calcium Chloride2×HCID 23687554MOPS sodium hydroxide

Produkt 1

HCID 9423-(1-Methylpyrrolidin-2-yl)pyridine

Versuchsvorschrift

The activity at pH 8.0 was determined using a buffer comprising 125 mM sodium chloride, 4.8 mM potassium chloride, 5.6 mM D-glucose, 1.2 mM calcium chloride, 1.2 mM potassium dihydrogen phosphate, 1.2 mM magnesium sulfate, and 25 mM tricine. The activity at pH 7.0 was further determined using a buffer comprising 125 mM sodium chloride, 4.8 mM potassium chloride, 5.6 mM D-glucose, 1.2 mM calcium chloride, 1.2 mM potassium dihydrogen phosphate, 1.2 mM magnesium sulfate, and 25 mM MOPS-NaOH.

Quellen und Nachweise

ORD-Eintrag
ord-b24988ae93094b4388681913d45969a0
Quelldatensatz
uspto-grants-2011_02
Patentnummer
US07892728B2

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