HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Dimethylaminopyridine → HCID 178469736, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Dimethylaminopyridine | HCID 21885 | — |
| Edukt | Ethyl 4-chloro-2-phenylpyrimidine-5-carboxylate | HCID 239537 | — |
| Edukt | HCID 178419079 | HCID 178419079 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | HCID 178469736 | HCID 178469736 | — |
Reaktionsschritte
Ethyl 4-chloro-2-phenyl-5-pyrimidinecarboxylate and N-tert-butoxycarbonyl-trans-1,4-cyclohexanediamine were reacted in ethanol in the presence of dimethylaminopyridine in the same manner as in Reference Example 3-49 to obtain N-tert-butoxycarbonyl-trans-4-(5-ethoxycarbonyl-2-phenyl-4-pyrimidinylamino)cyclohexylamine.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07160877B2 |
| Quelldatensatz | uspto-grants-2007_01 |
| ORD ID | ord-7cdd0e493b5a4360ae82acfd3eef692d |
| Quellennotiz | uspto-grants-2007_01 |