HCID 58786791, Verbindung → HCID 58786800, Verbindung
Reaktionsgleichung
[CH2:1]([N:3]([CH2:26][CH3:27])[CH2:4][CH2:5][O:6][C:7]1[CH:12]=[CH:11][C:10]([NH:13][C:14]2[N:19]=[C:18]([NH:20][CH2:21][CH3:22])[C:17]([N+:23]([O-])=O)=[CH:16][N:15]=2)=[CH:9][CH:8]=1)[CH3:2]>[Pd]>[NH2:23][C:17]1[C:18]([NH:20][CH2:21][CH3:22])=[N:19][C:14]([NH:13][C:10]2[CH:9]=[CH:8][C:7]([O:6][CH2:5][CH2:4][N:3]([CH2:26][CH3:27])[CH2:1][CH3:2])=[CH:12][CH:11]=2)=[N:15][CH:16]=1Komponenten
3
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
Hydrogenation of 2-[[4-[2-(diethylamino)ethoxy]phenyl]amino]-4-(ethylamino)-5-nitropyrimidine (from Example 2(7) above) over Pd/C gave the title compound as an oil.
Quellen und Nachweise
- ORD-Eintrag
- ord-623f4a28483e4ccbb56ec9d57c1f35aa
- Quelldatensatz
- uspto-grants-2007_01
- Patentnummer