Dimethyl Sulfate → p-tert-Butylanisole

HRID 1377012Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1377012
[C:1]([C:5]1[CH:10]=[CH:9][C:8]([OH:11])=[CH:7][CH:6]=1)([CH3:4])([CH3:3])[CH3:2].S(OC)(O[CH3:16])(=O)=O>>[C:1]([C:5]1[CH:6]=[CH:7][C:8]([O:11][CH3:16])=[CH:9][CH:10]=1)([CH3:4])([CH3:2])[CH3:3]

Komponenten

3

Edukt 2

HCID 6497Dimethyl SulfateHCID 73934-tert-Butylphenol

Produkt 1

HCID 94750p-tert-Butylanisole

Versuchsvorschrift

More specifically, the process for producing N-sec-butyl-4-tert-butyl-2,6-dinitroaniline comprises reacting 4-tert-butylphenol with dimethyl sulfate to produce 4-tert-butylanisole. The 4-tert-butylanisole is then reacted with nitrating agent to produce 2,6-dinitro-4-tert-butylanisole. The 2,6-dinitro-4-tert-butylanisole is then reacted with sec-butylamine to produce N-sec-butyl-4-tert-butyl-2,6-dinitroaniline.

Quellen und Nachweise

ORD-Eintrag
ord-a9ef234823074edd96c724bec71e0e6d
Quelldatensatz
uspto-grants-1997_09
Patentnummer
US05663441

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