HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1383825Erstellt: 26. Oktober 2026
Acetic Anhydride → (6-Methylpyridin-2-yl)methyl acetate
https://huagongshe.com/reaction/1383825
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Acetic Anhydride | HCID 7918 | — |
| Edukt | 2,6-Dimethylpyridine N-oxide | HCID 14083 | — |
| Produkt | (6-Methylpyridin-2-yl)methyl acetate | HCID 291137 | — |
Reaktionsschritte
Acetic anhydride (23 ml) was heated to 110° C. and 2,6-lutidine-N-oxide (20 g) was added dropwise over 1 hour. The solution was heated at 110° C. for five hours. After cooling, the crude mixture was distilled to yield 2-acetoxymethyl-6-methylpyridine (18.4 g, b.p. 110-120° C. @ 15 mmHg).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US06255305B1 |
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| Quelldatensatz | uspto-grants-2001_07 |
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| ORD ID | ord-9d21fda086014f35a60a392747967bee |
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| Quellennotiz | uspto-grants-2001_07 |
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