HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1384495Erstellt: 25. Oktober 2026
Phenylhydrazine → 2-(Phenylhydrazino)succinonitrile
https://huagongshe.com/reaction/1384495
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Phenylhydrazine | HCID 7516 | — |
| Edukt | Fumaronitrile | HCID 637930 | — |
| Produkt | 2-(Phenylhydrazino)succinonitrile | HCID 53865485 | 45% |
Reaktionsschritte
A mixture of phenylhydrazine (4.29 g) and fumaronitrile (3.1 g), where the phenylhydrazine served as a solvent, was heated at 75-80° C. for 20 hours. Purification by flash chromatography on silica gel and crystallization from dichloromethane/hexane gave the title compound (3.29 g, 45%), m.p. 97-98° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US06258973B1 |
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| Quelldatensatz | uspto-grants-2001_07 |
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| ORD ID | ord-f98160595e9245248d25f1cf5d0add2f |
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| Quellennotiz | uspto-grants-2001_07 |
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