Buspirone Hydrochloride → Buspirone

HRID 1402639

Reaktionsgleichung

Reaktionsgleichung von HRID 1402639
[CH:1]1[CH:2]=[N:3][C:4]([N:7]2[CH2:12][CH2:11][N:10]([CH2:13][CH2:14][CH2:15][CH2:16][N:17]3[C:27](=[O:28])[CH2:26][C:21]4([CH2:25][CH2:24][CH2:23][CH2:22]4)[CH2:20][C:18]3=[O:19])[CH2:9][CH2:8]2)=[N:5][CH:6]=1.Cl>CCO>[CH:1]1[CH:6]=[N:5][C:4]([N:7]2[CH2:12][CH2:11][N:10]([CH2:13][CH2:14][CH2:15][CH2:16][N:17]3[C:27](=[O:28])[CH2:26][C:21]4([CH2:22][CH2:23][CH2:24][CH2:25]4)[CH2:20][C:18]3=[O:19])[CH2:9][CH2:8]2)=[N:3][CH:2]=1

Komponenten

3

Edukt 1

HCID 36431Buspirone Hydrochloride

Produkt 1

HCID 2477Buspirone

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 702EthanolLösungsmittel

Versuchsvorschrift

0.2 grams of Phospholipin 90 were dissolved in 2.5 grams EtOH; to this solution 0.02 grams of Vitamin E were added and mixed to obtain a clear system. To this system, 0.2 grams of buspirone HCl dissolved in 7.08 grams DDW were slowly added under constant stirring at room temperature in Heidolph mixer (700 rpm). The obtained system was stirred for additional 5 minutes.

Aufarbeitung

  1. additionmixed
  2. customto obtain a clear system
  3. additionwere slowly added
  4. stirringThe obtained system was stirred for additional 5 minutes

Quellen und Nachweise

ORD-Eintrag
ord-bf8638285ae54532a2da69bf1f4e4edb
Quelldatensatz
uspto-grants-2014_12
Patentnummer
US08911751B2

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