2-(Dibutylamino)ethanol → N,N-Dibutyl-N-(2-hydroxyethyl)butan-1-aminium chloride

Beteiligte Stoffe

Reaktionsschritte

70 mmol of 2-(dibutylamino) ethanol, 75 mmol of 1-chlorobutane, and 50 g of ethanol were mixed under N2 atmosphere, and made to react at 80 degrees C. for 8 hours under reflux condition. The ethanol and extra 1-chlorobutane were distilled away therefrom by reducing pressure to produce 70 mmol of (2-hydroxyethyl)tributylammonium chloride.

Herkunft & Nachweise