反应详情

70 mmol of 2-(dibutylamino) ethanol, 75 mmol of 1-chlorobutane, and 50 g of ethanol were mixed under N2 atmosphere, and made to react at 80 degrees C. for 8 hours under reflux condition. The ethanol and extra 1-chlorobutane were distilled away therefrom by reducing pressure to produce 70 mmol of (2-hydroxyethyl)tributylammonium chloride.

1. customto react at 80 degrees C
2. temperaturefor 8 hours under reflux condition
3. distillationThe ethanol and extra 1-chlorobutane were distilled away