HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Potassium Hydroxide → 3-Hydroxy-3-phenylpropanoic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Potassium Hydroxide | HCID 14797 | — |
| Edukt | Ethyl 3-phenylhydracrylate, (+-)- | HCID 99818 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | 3-Hydroxy-3-phenylpropanoic acid | HCID 92959 | — |
Reaktionsschritte
Ethyl 3-hydroxy-3-phenylpropanoate (19 g, 0.1 mole) was refluxed in a solution of KOH (10 g, 0.2 mole) in ethanol for two hours. The solvent was removed in vacuo and the residue was dissolved in H2O. The H2O solution was extracted with ethyl ether, then acidified with 37% hydrochloric acid. The oily product was extracted out with chloroform and the chloroform was removed in vacuo to yield 10 g (62.5%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04002660 |
| Quelldatensatz | uspto-grants-1977_01 |
| ORD ID | ord-cdcbffa4f09742e9845325766a34354c |
| Quellennotiz | uspto-grants-1977_01 |