HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
N-Methyl-D-glucamine → N-Methyl-D-glucamine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | N-Methyl-D-glucamine | HCID 8567 | — |
| Edukt | Amoxicillin Trihydrate | HCID 62883 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | N-Methyl-D-glucamine | HCID 8567 | — |
| Produkt | Amoxicillin | HCID 33613 | — |
Reaktionsschritte
3 G. of N-methyl-D-glucamine are added to a suspension of 6 g. of amoxicillin trihydrate in 80 ml. of water and stirred at 5° C. Insoluble material is fitered off under suction and the resulting filtrate is lyophilized. There is thus obtained the N-methyl-D-glucamine salt of amoxicillin. Melting point: about 160° C. (decomposition). [α]D25 = + 133° (c =1 in water).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04005214 |
| Quelldatensatz | uspto-grants-1977_01 |
| ORD ID | ord-4bb8520051cd446fad35e01eb9c612fa |
| Quellennotiz | uspto-grants-1977_01 |