2,3-Dichloro-1,3-butadiene → Formaldehyde

HRID 1416149

Reaktionsgleichung

Reaktionsgleichung von HRID 1416149
S([O-])([O:4][CH2:5]CCCCCCCCCCC)(=O)=O.[Na+].ClC(C(Cl)=C)=C.[C:25]1([CH:32]=[CH:31][CH:30]=[C:28]([OH:29])[CH:27]=1)[OH:26].[CH2:33]=[O:34]>O>[C:25]1([CH:32]=[CH:31][CH:30]=[C:28]([OH:29])[CH:27]=1)[OH:26].[CH2:5]=[O:4].[C:25]1([CH:32]=[CH:31][CH:30]=[C:28]([OH:29])[CH:27]=1)[OH:26].[CH2:33]=[O:34]

Komponenten

7

Edukt 3

HCID 154472,3-Dichloro-1,3-butadieneHCID 159980Resorcinol-formaldehyde resinHCID 3423265Sodium Lauryl Sulfate

Produkt 3

HCID 712FormaldehydeHCID 5054ResorcinolHCID 159980Resorcinol-formaldehyde resin

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Versuchsvorschrift

18.0 g of sodium lauryl sulfate (Emar 2F Needle (30% concentration), manufactured by Kao Corporation) was added as a surfactant to 295 g of the above 2,3-dichlrobutadiene homopolymer latex (2), and the mixture was thoroughly stirred until it became uniform. Then, 264.4 g of water was added thereto, and 656.4 g of the resorcinol/formaldehyde mixed liquid prepared as described above, was mixed thereto. The mixture was left to stand and aged at 23° C. for 24 hours to obtain a resorcinol/formaldehyde/latex mixed liquid (the weight ratio of the latex solid content to the sum of resorcinol and formaldehyde: 1/0.86, total amount of surfactant: 0.74 wt %).

Aufarbeitung

  1. additionwas mixed
  2. waitThe mixture was left

Quellen und Nachweise

ORD-Eintrag
ord-33ccf3d8a116452a9930165ca488d1a2
Quelldatensatz
uspto-grants-1999_06
Patentnummer
US05912079

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