HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methanol → Monomethyl maleate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methanol | HCID 887 | — |
| Edukt | Maleic Anhydride | HCID 7923 | — |
| Produkt | Monomethyl maleate | HCID 5354456 | — |
Reaktionsschritte
The same procedure as that of process (I) of Example 1 was conducted to obtain a 50% by weight methanol solution of (A1). In the same manner, to a 1 liter flask were added 24.00 g of maleic anhydride and 39.68 g of methanol, and the resulting mixture was stirred under reflux in a water bath kept at 90° C. Thirty minutes after initiation of the stirring, solid components disappeared, 3 hours after, the temperature was lowered to room temperature to obtain a 50% by weight methanol solution of maleic monomethyl ester.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05914385 |
| Quelldatensatz | uspto-grants-1999_06 |
| ORD ID | ord-cc36d2f1e923404c8fb8aef00087bf94 |
| Quellennotiz | uspto-grants-1999_06 |