Isoprene → Isoprene hydroxypropyl-beta-cyclodextrin

HRID 1420466

Reaktionsgleichung

Reaktionsgleichung von HRID 1420466
[CH3:1][CH:2]([OH:105])[CH2:3][O:4][CH2:5][C@H:6]1[O:11][C@@H:10]2[O:12][C@H:13]3[C@H:18]([OH:19])[C@@H:17]([OH:20])[C@@H:16]([O:21][C@H:22]4[C@H:27]([OH:28])[C@@H:26]([OH:29])[C@@H:25]([O:30][C@H:31]5[C@H:36]([OH:37])[C@@H:35]([OH:38])[C@@H:34]([O:39][C@H:40]6[C@H:45]([OH:46])[C@@H:44]([OH:47])[C@@H:43]([O:48][C@H:49]7[C@H:54]([OH:55])[C@@H:53]([OH:56])[C@@H:52]([O:57][C@H:58]8[C@H:64]([OH:65])[C@@H:63]([OH:66])[C@@H:61]([O:62][C@H:7]1[C@H:8]([OH:104])[C@H:9]2[OH:103])[O:60][C@@H:59]8[CH2:67][O:68][CH2:69][CH:70]([OH:72])[CH3:71])[O:51][C@@H:50]7[CH2:73][O:74][CH2:75][CH:76]([OH:78])[CH3:77])[O:42][C@@H:41]6[CH2:79][O:80][CH2:81][CH:82]([OH:84])[CH3:83])[O:33][C@@H:32]5[CH2:85][O:86][CH2:87][CH:88]([OH:90])[CH3:89])[O:24][C@@H:23]4[CH2:91][O:92][CH2:93][CH:94]([OH:96])[CH3:95])[O:15][C@@H:14]3[CH2:97][O:98][CH2:99][CH:100]([OH:102])[CH3:101].[CH2:106]=[CH:107][C:108](=[CH2:110])[CH3:109]>>[CH2:106]=[CH:107][C:108](=[CH2:109])[CH3:110].[CH3:71][CH:70]([OH:72])[CH2:69][O:68][CH2:67][C@H:59]1[O:60][C@@H:61]2[O:62][C@H:7]3[C@H:8]([OH:104])[C@@H:9]([OH:103])[C@@H:10]([O:12][C@H:13]4[C@H:18]([OH:19])[C@@H:17]([OH:20])[C@@H:16]([O:21][C@H:22]5[C@H:27]([OH:28])[C@@H:26]([OH:29])[C@@H:25]([O:30][C@H:31]6[C@H:36]([OH:37])[C@@H:35]([OH:38])[C@@H:34]([O:39][C@H:40]7[C@H:45]([OH:46])[C@@H:44]([OH:47])[C@@H:43]([O:48][C@H:49]8[C@H:54]([OH:55])[C@@H:53]([OH:56])[C@@H:52]([O:57][C@H:58]1[C@H:64]([OH:65])[C@H:63]2[OH:66])[O:51][C@@H:50]8[CH2:73][O:74][CH2:75][CH:76]([OH:78])[CH3:77])[O:42][C@@H:41]7[CH2:79][O:80][CH2:81][CH:82]([OH:84])[CH3:83])[O:33][C@@H:32]6[CH2:85][O:86][CH2:87][CH:88]([OH:90])[CH3:89])[O:24][C@@H:23]5[CH2:91][O:92][CH2:93][CH:94]([OH:96])[CH3:95])[O:15][C@@H:14]4[CH2:97][O:98][CH2:99][CH:100]([OH:102])[CH3:101])[O:11][C@@H:6]3[CH2:5][O:4][CH2:3][CH:2]([OH:105])[CH3:1]

Komponenten

3

Edukt 2

HCID 6557IsopreneHCID 140496892-Hydroxypropyl-Beta-Cyclodextrin

Produkt 1

HCID 86755429Isoprene hydroxypropyl-beta-cyclodextrin

Versuchsvorschrift

15 ml of 20% hydroxypropyl-β-cyclodextrin solution were mixed with 2 ml of isoprene at 10° C., ultrasounded for 3 minutes in the ultrasonic bath and then incubated for 26 hours. The resulting complex remained partly in solution and precipitated partly as a white deposit.

Aufarbeitung

  1. waitincubated for 26 hours
  2. customprecipitated partly as a white deposit

Quellen und Nachweise

ORD-Eintrag
ord-76aba479a3714214a9f0fa494cf17bcf
Quelldatensatz
uspto-grants-2000_06
Patentnummer
US06071496

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