2-Aminobenzonitrile → N-(2-cyanophenyl)cyclohexanecarboxamide
Reaktionsgleichung
F[C:2](F)(F)[C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[NH:9][C:10]([CH:12]1[CH2:17][CH2:16][CH2:15][CH2:14][CH2:13]1)=[O:11].C(C1C=CC=CC=1N)#[N:21]>>[C:2]([C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[NH:9][C:10]([CH:12]1[CH2:17][CH2:16][CH2:15][CH2:14][CH2:13]1)=[O:11])#[N:21]Komponenten
3
Versuchsvorschrift
This compound was prepared following the procedure described for compound 26A in example 26, except that 2-cyanoaniline was used in place of 2-trifluoromethylaniline. Yield 75%. M.p. 135-137° C.
Aufarbeitung
- customThis compound was prepared
Quellen und Nachweise
- ORD-Eintrag
- ord-f293dc1a344b4a669639b9bd4a615eed
- Quelldatensatz
- uspto-grants-2000_06
- Patentnummer
- US06071920
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