HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
6-Methoxy-3,4-dihydronaphthalen-2-yl trifluoromethanesulfonate → 7-Methoxy-3-(4-methoxy-2-nitrophenyl)-1,2-dihydronaphthalene
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 6-Methoxy-3,4-dihydronaphthalen-2-yl trifluoromethanesulfonate | HCID 15330256 | — |
| Edukt | Tributyl(4-methoxy-2-nitrophenyl)tin | HCID 23087474 | — |
| Produkt | 7-Methoxy-3-(4-methoxy-2-nitrophenyl)-1,2-dihydronaphthalene | HCID 23087141 | 73,2% |
Reaktionsschritte
Synthesized from 6-methoxy-3,4-dihydronaphthalen-2-yl trifluoromethanesulfonate (2.3 g) and tributyl(4-methoxy-2-nitrophenyl)tin (3.9 g) according to an analogous synthetic method to Preparation Example 77, the title compound (1.7 g) was obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07612114B2 |
| Quelldatensatz | uspto-grants-2009_11 |
| ORD ID | ord-93695c5539284e51b554a25583905b0f |
| Quellennotiz | uspto-grants-2009_11 |