Ammonia → HCID 3046207, Verbindung
Reaktionsgleichung
[NH2-:1].[Na+].N.[Na].[CH2:5]([C:8]([CH2:12][CH2:13][CH3:14])(Cl)[C:9]#[CH:10])[CH2:6][CH3:7]>C(OCC)C>[CH2:5]([C:8]([NH2:1])([CH2:12][CH2:13][CH3:14])[C:9]#[CH:10])[CH2:6][CH3:7]Komponenten
6
Edukt 4
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
To a suspension of sodium amide in liquid ammonia, prepared from 6.9 g of sodium and 250 ml of liquid ammonia, were added 17 g of 1,1-di-n-propyl-1-chloro-2-propyne in 50 ml of anhydrous ethyl ether. The operation of adding the chlorinated derivative lasted one hour. Stirring of the mixture was maintained for 2 hours and then 300 ml of anhydrous ethyl ether were added.
Aufarbeitung
- additionThe operation of adding the chlorinated derivative
- temperaturewas maintained for 2 hours
Quellen und Nachweise
- ORD-Eintrag
- ord-ac5ba1381e5741808c66b4cc76ef940a
- Quelldatensatz
- uspto-grants-1977_11
- Patentnummer
- US04057644
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