Benzaldehyde → N-Benzylidene(piperidin-4-yl)methanamine

HRID 1444096

Reaktionsgleichung

Reaktionsgleichung von HRID 1444096
[CH:1](=O)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[NH2:9][CH2:10][CH:11]1[CH2:16][CH2:15][NH:14][CH2:13][CH2:12]1>C1(C)C=CC=CC=1>[NH:14]1[CH2:15][CH2:16][CH:11]([CH2:10][N:9]=[CH:1][C:2]2[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=2)[CH2:12][CH2:13]1

Komponenten

4

Edukt 2

HCID 240BenzaldehydeHCID 235274-(Aminomethyl)piperidine

Produkt 1

HCID 11820173N-Benzylidene(piperidin-4-yl)methanamine

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 1140TolueneLösungsmittel

Versuchsvorschrift

Benzaldehyde (4.6 g; 0.044 mol) was added dropwise to a solution of 4-aminomethylpiperidine (5.0 g; 0.044 mol) in toluene (20 ml). The solution thus obtained was stirred for 3 h at room temperature. Then the solvent was removed by evaporation at reduced pressure and the residue was taken up twice with toluene to give the desired product that was used as such without further purification.

Aufarbeitung

  1. customThe solution thus obtained
  2. customThen the solvent was removed by evaporation at reduced pressure

Quellen und Nachweise

ORD-Eintrag
ord-5924d5348ad944b5b28619e072e9943f
Quelldatensatz
uspto-grants-2010_02
Patentnummer
US07662836B2

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