HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Benzaldehyde → N-Benzylidene(piperidin-4-yl)methanamine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Benzaldehyde | HCID 240 | — |
| Edukt | 4-(Aminomethyl)piperidine | HCID 23527 | — |
| Lösungsmittel | Toluene | HCID 1140 | — |
| Produkt | N-Benzylidene(piperidin-4-yl)methanamine | HCID 11820173 | — |
Reaktionsschritte
Benzaldehyde (4.6 g; 0.044 mol) was added dropwise to a solution of 4-aminomethylpiperidine (5.0 g; 0.044 mol) in toluene (20 ml). The solution thus obtained was stirred for 3 h at room temperature. Then the solvent was removed by evaporation at reduced pressure and the residue was taken up twice with toluene to give the desired product that was used as such without further purification.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07662836B2 |
| Quelldatensatz | uspto-grants-2010_02 |
| ORD ID | ord-5924d5348ad944b5b28619e072e9943f |
| Quellennotiz | uspto-grants-2010_02 |