HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
5-Bromotryptamine → N-(alpha-ethyl-delta-hydroxy-valeroyl)-5-bromo-tryptamine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 5-Bromotryptamine | HCID 77158 | — |
| Edukt | 2H-Pyran-2-one, 3-ethyltetrahydro- | HCID 3656318 | — |
| Lösungsmittel | O-Xylene | HCID 7237 | — |
| Produkt | N-(alpha-ethyl-delta-hydroxy-valeroyl)-5-bromo-tryptamine | HCID 13241177 | 80% |
Reaktionsschritte
0.48 g. (2.0 mmoles) of 5-bromo-tryptamine and 0.30 g. (2.3 mmoles) of 2-ethyl-pentanolide are dissolved in 5 ml. of abs. xylene, and the solution is refluxed for 4 hours. The reaction mixture is evaporated in vacuo, the residue is triturated twice with 3 ml. each of petroleum ether, thereafter it is dried in a desiccator. 0.59 g. (80%) of N-(α-ethyl-δ-hydroxy-valeroyl)-5-bromo-tryptamine are obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04315011 |
| Quelldatensatz | uspto-grants-1982_02 |
| ORD ID | ord-714ca3903f054c399b0c7d7391711205 |
| Quellennotiz | uspto-grants-1982_02 |