Zurück
HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1446994Erstellt: 26. Oktober 2026

5-Bromotryptamine → N-(alpha-ethyl-delta-hydroxy-valeroyl)-5-bromo-tryptamine

https://huagongshe.com/reaction/1446994

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt5-BromotryptamineHCID 77158—
Edukt2H-Pyran-2-one, 3-ethyltetrahydro-HCID 3656318—
LösungsmittelO-XyleneHCID 7237—
ProduktN-(alpha-ethyl-delta-hydroxy-valeroyl)-5-bromo-tryptamineHCID 1324117780%

Reaktionsschritte

0.48 g. (2.0 mmoles) of 5-bromo-tryptamine and 0.30 g. (2.3 mmoles) of 2-ethyl-pentanolide are dissolved in 5 ml. of abs. xylene, and the solution is refluxed for 4 hours. The reaction mixture is evaporated in vacuo, the residue is triturated twice with 3 ml. each of petroleum ether, thereafter it is dried in a desiccator. 0.59 g. (80%) of N-(α-ethyl-δ-hydroxy-valeroyl)-5-bromo-tryptamine are obtained.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04315011
Quelldatensatzuspto-grants-1982_02
ORD IDord-714ca3903f054c399b0c7d7391711205
Quellennotizuspto-grants-1982_02