Water → HCID 22097227, Verbindung
Reaktionsgleichung
[Cl:1][C:2]1[CH:7]=[C:6]([NH:8]C(=O)C)[C:5]([NH:12]C(=O)C)=[CH:4][C:3]=1[N:16]1[CH:20]=[CH:19][CH:18]=[CH:17]1.[OH-].[K+].O>C(O)CO>[Cl:1][C:2]1[CH:7]=[C:6]([NH2:8])[C:5]([NH2:12])=[CH:4][C:3]=1[N:16]1[CH:20]=[CH:19][CH:18]=[CH:17]1Komponenten
5
Edukt 3
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
A solution 1.4 g (4.8 mmol) of N-(2-chloro-4,5-diacetamidophenyl)pyrrole and 0.4 g (9.8 mmol) of potassium hydroxide in 25 ml of ethylene glycol was stirred at 60° C. for 30 minutes. The reaction mixture was then poured into water, extracted with ethyl acetate and worked up.
Aufarbeitung
- extractionextracted with ethyl acetate
Quellen und Nachweise
- ORD-Eintrag
- ord-b5aeb035bbc04359a7ae943f1de7c367
- Quelldatensatz
- uspto-grants-1998_12
- Patentnummer
- US05852017
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