Reaktionsgleichung
[Na].ClC1C(S)=C(Cl)C(Cl)=C(Cl)C=1Cl.[N+]([O-])(O)=O.[S:18](=[O:22])(=[O:21])([OH:20])[OH:19].[S:23](=[O:26])(=[O:25])=[O:24]>>[OH:21][S:18]([OH:22])(=[O:20])=[O:19].[O:24]=[S:23](=[O:26])=[O:25]Komponenten
6
Versuchsvorschrift
reacting this sodium salt of pentachlorothiophenol with a mixed nitration acid comprising nitric acid and sulfuric acid (and, preferably, sulfur trioxide to form oleum) at a temperature from about 35° C. to about 110° C. to form pentachloronitrobenzene, the nitric acid being in molar excess of the pentachlorothiophenol.
Quellen und Nachweise
- ORD-Eintrag
- ord-ef5d4417de7a4c94a97e21416b1302a2
- Quelldatensatz
- uspto-grants-1984_07
- Patentnummer
- US04461918
Verknüpfte Notizen
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