Dibenzylamine → N,N-Dibenzyl-3-oxo-4-azaandrost-5-ene-17beta-carboxamide

HRID 1463940

Reaktionsgleichung

Reaktionsgleichung von HRID 1463940
[O:1]=[C:2]1[CH2:19][CH2:18][C@@:17]2([CH3:20])[C:4](=[CH:5][CH2:6][C@@H:7]3[C@@H:16]2[CH2:15][CH2:14][C@@:12]2([CH3:13])[C@H:8]3[CH2:9][CH2:10][C@@H:11]2[C:21]([OH:23])=O)[NH:3]1.[CH2:24]([NH:31][CH2:32][C:33]1[CH:38]=[CH:37][CH:36]=[CH:35][CH:34]=1)[C:25]1[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=1>>[CH2:32]([N:31]([CH2:24][C:25]1[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=1)[C:21]([C@H:11]1[CH2:10][CH2:9][C@H:8]2[C@H:7]3[C@H:16]([CH2:15][CH2:14][C@:12]12[CH3:13])[C@:17]1([CH3:20])[C:4]([NH:3][C:2](=[O:1])[CH2:19][CH2:18]1)=[CH:5][CH2:6]3)=[O:23])[C:33]1[CH:38]=[CH:37][CH:36]=[CH:35][CH:34]=1

Komponenten

3

Edukt 2

HCID 7656DibenzylamineHCID 4754473-Oxo-4-aza-5-androstene-17beta-carboxylic acid

Produkt 1

HCID 67750691N,N-Dibenzyl-3-oxo-4-azaandrost-5-ene-17beta-carboxamideAusbeute 71 %

Versuchsvorschrift

The title compound was prepared in a yield of 71% in a similar manner to that described in Example 1 by reacting 3-oxo-4-azaandrost-5-ene-17β-carboxylic acid and N,N-dibenzylamine.

Quellen und Nachweise

ORD-Eintrag
ord-96d971e536074cf6b8cc2a89f900042a
Quelldatensatz
uspto-grants-1994_04
Patentnummer
US05302621

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