HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
M-Cresol → HCID 178484374, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | M-Cresol | HCID 342 | — |
| Edukt | Dimethylcyanamide | HCID 15112 | — |
| Edukt | 5-Fluoro-[1,1'-biphenyl]-2-amine hydrochloride | HCID 19089218 | — |
| Produkt | HCID 178484374 | HCID 178484374 | — |
Reaktionsschritte
A mixture of 2-amino-5-fluorobiphenyl hydrochloride (3.6 g), N,N-dimethylcyanamide (1.68 g) and m-cresol (25 ml) was heated at 90°-95° C. for 8 hours to give N-(5-fluoro-2-biphenylyl)-N',N'-dimethylguanidine (m.p. 160°-161° C.) which was recrystallised from hexane.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05302720 |
| Quelldatensatz | uspto-grants-1994_04 |
| ORD ID | ord-20fb8c4e79754dc3a355821d79cc8c76 |
| Quellennotiz | uspto-grants-1994_04 |