Vinyl chloroformate → HCID 59601719, Verbindung

HRID 1464861Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1464861
[CH3:1][O:2][NH:3][C:4](=[O:7])[CH:5]=[CH2:6].[CH:8]([O:10][C:11](Cl)=[O:12])=[CH2:9]>>[CH:8]([O:10][C:11](=[O:12])[N:3]([O:2][CH3:1])[C:4](=[O:7])[CH:5]=[CH2:6])=[CH2:9]

Komponenten

3

Edukt 2

HCID 78808Vinyl chloroformateHCID 13531445N-Methoxyprop-2-enamide

Produkt 1

HCID 59601719HCID 59601719, Verbindung

Versuchsvorschrift

The synthesis was carried out analogously to synthesis example 8 using N-methoxy-acrylamide and chloroformic acid vinyl ester. Purification by column chromatography on silica gel (PE:EE=9:1) yielded 1.6 g (91% of th.) of the title compound as a colorless liquid.

Aufarbeitung

  1. customPurification by column chromatography on silica gel (PE:EE=9:1)

Quellen und Nachweise

ORD-Eintrag
ord-5457b3292eac4bc197a3beacfcc105ba
Quelldatensatz
uspto-grants-2015_04
Patentnummer
US08999323B2

Notizen zur Reaktion

Wird geladen…