Ethanol → L-Carnitine Vinpocetine

HRID 1484009

Reaktionsgleichung

Reaktionsgleichung von HRID 1484009
[OH:1][C@H:2]([CH2:8][C:9](=[O:11])[O-:10])[CH2:3][N+:4]([CH3:7])([CH3:6])[CH3:5].[CH3:12][CH2:13][C@:14]12[CH:30]=[C:29]([C:31]([O:33][CH2:34][CH3:35])=[O:32])[N:28]3[C:20]4=[C:21]([CH2:36][CH2:37][N:18]([C@@H:19]14)[CH2:17][CH2:16][CH2:15]2)[C:22]1[CH:23]=[CH:24][CH:25]=[CH:26][C:27]=13.C(O)C.C(OC(C1C=CC(O)=CC=1)=O)C>OCC(CO)O>[OH:1][C@H:2]([CH2:8][C:9](=[O:10])[O-:11])[CH2:3][N+:4]([CH3:7])([CH3:5])[CH3:6].[CH3:12][CH2:13][C@:14]12[CH:30]=[C:29]([C:31]([O:33][CH2:34][CH3:35])=[O:32])[N:28]3[C:20]4=[C:21]([CH2:36][CH2:37][N:18]([C@@H:19]14)[CH2:17][CH2:16][CH2:15]2)[C:22]1[CH:23]=[CH:24][CH:25]=[CH:26][C:27]=13

Komponenten

6

Edukt 4

HCID 702EthanolHCID 8434EthylparabenHCID 10917(-)-CarnitineHCID 443955Vinpocetine

Produkt 1

HCID 86298728L-Carnitine Vinpocetine

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 753GlycerolLösungsmittel

Reaktionsbedingungen

Temperatur
55 °C

Versuchsvorschrift

Process: Take L-carnitine and vinpocetine, add into ethanol and boil to completely dissolution, add ethylparaben and stir, and add defined amount of glycerin and stir uniformly, and then slowly add the solution into glycerinated gelatin substrate to preserve heat for later use. Add polysorbate and stir uniformly, and then slowly stir the solution and add it into the said glycerinated gelatin substrate, stir well and preserve the heat at 55° C., and affuse into the membrane, and cool them down.

Aufarbeitung

  1. dissolutionboil to completely dissolution
  2. additionadd
  3. stirringstir uniformly
  4. additionslowly add the solution
  5. temperatureto preserve heat for later use
  6. stirringslowly stir the solution
  7. additionadd it into the
  8. stirringstir well
  9. temperaturecool them down

Quellen und Nachweise

ORD-Eintrag
ord-0d90cf60a49f4759bb6288e96dc232f1
Quelldatensatz
uspto-grants-2016_08
Patentnummer
US09421181B2

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